GCMS calibration results for sample AE02092, March 2002

Quantitation Report (QT Reviewed) 2 2 K K O Data File C : \MSDCHEM\ 1\DATA\ 0 318 0 2 \ CAL4 0 . D Vial: 2 O 3 Acq On Sample 19 Mar 2002 3:00 am Operator: Inst : McLean Instrumen co — O 1 Mise Multiplr: 1.00 O O C O MS Integration Params: BENZO.P CT O O Quant Time: Mar 19 21:41 2002 Quant Results File: 5080302.RES o' C U 00 o co Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) — 0 Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 O o Response via : Initial Calibration o C Abundance TIC: CAL40.D 3 o D

1.5e+07

1.4e+07 Q to 73 § £

1 1.3e+07 20 6 b 0) § £ § O & 5 0 - 5 6 s. CD i

5 Oto § 5 88 z 5 CD 1.2e+07 73 > S s 2 s £ 2 o ( g i 73 £ 6 it 4S. • O

i‘s £ $co £ to ( 5 8 48 6 8 2 5 9 N a « ( 1.1e+07 0) 8 6 X tE 8 o IIo P If 5 g S' 33 J- 8 S 5 00 S 8 s . N 5 8. i 4 8 g 0 Fo C °e 9 1e+07 is d £ $ 8 8 88 88 58 a 2O 9000000 85 as $8 HSi 8 | $ D

1 £ £ $

8000000 t F !1if 33 i 8 0 5 3 1 a 8

7000000 e -2 g p 8 o g $ x £ . g 58 8 4 l 1 £ & $ 1 5 S “ 8 2 m8 I J w o

6000000 f $1 n § □ G a £ N & g 2 i5 S

5000000 x o § ti c- 0

£3 j s cE .U —Q

ia i5 F 4000000 z — 0 co

3000000

2000000

1000000 — Time-> 0 6.00 1 ■1 8.00 1 10.00 IP 12.00 14.00 116.00A1 18.00 20.00 4r ------- 22.00 24.00 26.00 PIr 1 T — । T -i- 28.00 30.00 32.00 34.00 36.00 — 1 38.00

CAL40.D 5080302.M Wed Mar 20 03:17:56 2002 Page 3