GCMS analysis results for sample AE02567, March 2002

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Laboratory report documenting GCMS analysis of sample AE02567 conducted on March 25, 2002, identifying other unknown compounds.

NYC-WTC_000038901–000038910

Folder label: “GCMS X 3/4/02 A 3/20/02”

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Data File : C:\HPCHEM\1\DATA\MAR1902\2567.D Vial: 22 Acq On : 21 Mar 2002 1:42 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 13:57 2002 <Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 446752 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 1720013 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.21 164 928961 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1358516 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 818620 20.00 ug/1 -0.13 44) Perylene-dl2 37.97 264 505818 20.00 ug/1 -0.15

System Monitoring Compounds 37) 2,4-DDD 30.73 235 83006 8.41 ug/mL 0.24 Spiked Amount 5.000 Recovery = 168.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.48 74 215 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.97 128 401 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.51 165 186 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 2567.D GCMS0308.M Thu Mar 21 13:58:15 2002 Page 1

NYC-WTC_000038903

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GCMS analysis results for sample AE02568, March 2002 · Box DEP Box 23

NYC-WTC_000038891

Laboratory report documenting GCMS analysis of sample AE02568 conducted on March 25, 2002, identifying other unknown compounds.

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