GCMS Method 608 data sheet fragment, March 2002

NYC 9/11 Public Portal Document

DFTPP

f Data File C: \HPCHEM\1\DATA\MAR1902\DFTPP2 .D Vial: 1 Acq On 20 Mar 2002 8:58 am Operator : Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP2.D 2500000-

2000000-

1500000

1000000

500000 —........ —.......... . .... i ■ 0- Time->__ 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 _ Abundance Average of 26.822 to 26.868 min.: DFTPP2.D 198 150000

442 100000- 69 255 127 51 50000 110 275 224 93 0 38 + J ——1—++ 4.14115416710. 11—42. 1 'i 1' j I।T j 1 J । | 1111111111 .1,. 296310323 . 352365 383 403 423 TT T r r r | I I 1 -I [ '> T I 'I i’ । ■ । r । j । i I t । । i । . IT 1 . I |‘1 ... I trr m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.822 to 26.868 min.

Target Rel. to Lower Upper Rel. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 37.6 58803 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 48.8 76397 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 44.4 69471 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 156540 PASS 199 198 5 9 6.7 10527 PASS 275 198 10 30 22.0 34504 PASS 365 198 1 100 2.3 3678 PASS 441 443 0.01 100 93.8 18220 PASS 442 198 40 110 64.7 101248 PASS 443 442 17 23 19.2 19431 PASS

DFTPP2.D GCMS0308.M Thu Mar 21 13:36:39 2002

NYC-WTC_000038751