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GCMS analysis results for sample AE01462, Feb 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.

NYC-WTC_000038642–000038656

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

P Quantitation Report (QT Reviewed) 03 Data File : C:\HPCHEM\l\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 22 9:23 2002 iQuant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.73 178 187 N.D. 34) Anthracene 25.73 178 187 N.D. 35) Di-n-butylphthalate 27.69 149 6314 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 30.11 202 209 N.D. 40) Butylbenzylphthalate 32.23 149 1177 N.D. 41) Benzo(a)anthracene 33.81 228 1667 N.D. 42) Bis(2-ethylhexyl)phthalate 34.01 149 10978 0.25 ug/1 # 92 43) Chrysene 33.81 228 1667 N.D. 45) Di-n-Octylphthalate 35.75 149 2222 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38 .09 252 1827 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1462.D GCMS0308.M Mon Mar 25 08:24:07 2002 Page 2

NYC-WTC_000038643

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NYC-WTC_000038643Source: NYC Law Department, mirrored locally

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