GCMS quantitation results for sample AE04028, March 2002

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Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.

NYC-WTC_000038511–000038520

Folder label: “GCMS X 2/25/02 A 3/23/02”

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NYC 9/11 Public Portal Document

N Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2202\4028.D Vial: 34 Acq On : 24 Mar 2002 2:39 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 9:54 2002 ।Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS03 8

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 421812 20.00 ug/1 -0.09 10) Naphthalene-d8 15.90 136 1714113 20.00 ug/1 -0.10 17) Acenaphthene-diO 21.22 164 959199 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1423689 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 913889 20.00 ug/1 -0.13 44) Perylene-dl2 37.97 264 543767 20.00 ug/1 -0.15

System Monitoring Compounds 37) 2,4-DDD 3 0.74 235 85244 S.14 , 8.24 ug/mL 0.24 Spiked Amount 5.000 Recovery 164.80% jo-“b Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.95 128 544 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.69 149 909 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 4028.D GCMS0308.M Tue Mar 26 09:58:25 2002 Page 1

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