NYC 9/11 Public Portal Document
Data File C:\MSDCHEM\l\DATA\022802\03441.D Vial: 28
Acq On 1 Mar 2002 10:42 am Operator: McLean
* Sample MS CSAN FB Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: BENZO.P
Quant Time: Mar 13 06:51:19 2002 Quant Results File: 5080202.RES
Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Last Update : Mon Feb 25 19:17:14 2002
Response via : Initial Calibration
DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 9.58 150 1022535 20.00 ug/L 0.00
10) Naphthalene-d8 13.05 136 2733382 20.00 ug/L 0.00
17) Acenaphthene-dl0 18.16 164 1510029 20.00 ug/L 0.00
29) Phenanthrene-dlO 22.52 188 2270647 20.00 ug/L 0.00
38) Chrysene-dl2 30.33 240 1950621 20.00 ug/L -0.03
44) Perylene-dl2 34.20 264 1229795 20.00 ug/L -0.02
System Monitoring Compounds
37) 2,4-ddd surr 27.46 235 183556 5.09 ug/L G .00
Spiked Amount 5.000 Recovery = 101.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 3.27 74 6051 0.20 ug/L 100
3) bis(2-chloroethyl) ether 0.00 93 0 N.D.
4) 1,3 - Dichlorobenze 0.00 146 0 N.D.
5) 1,4 - Dichlorobenzene 0.00 146 0 N.D.
6) 1,2 - Dichlorobenzene 0.00 146 0 N.D.
7) 2,2 ' - oxybis (l-Chloropr 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 18.16 165 193618 9.22 ug/L #
22) Acenaphthylene
23) Acenaphthene
24) 2,4-Dinitrotoluene
0.00
0.00
0.00
152
153
165
0
0
0
N.D.
N.D.
N.D.
25X
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
30) N-Nitrosodiphenylamine 0.00 169 0 N.D.
31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D.
32) Hexachlorobenzene 0.00 284 0 N.D.
33) Phenanthrene 0.00 178 0 N.D.
34) Anthracene 0.00 178 0 N.D.
35) Di-n-butylphthalate 24.66 149 3685 0.02 ug/L 79
36) Fluoranthene 0.00 202 0 N.D.
39) Pyrene 0.00 202 0 N.D.
40) Butylbenzylphthalate 0.00 149 0 N.D.
41) Benzo (a) antracene 0.00 228 0 N.D. d
42) Bis (2-ethylhexyl) phthala 30.94 149 103801 1.17 ug/L 97
43) Chrysene 0.00 228 0 N.D. d
45) Di-n-Octylphthalate 0.00 149 0 N.D.
46) Benzo (b) fluoranthene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration
03441.D 5080202.M Wed Mar 13 06:52:00 2002 Page 1
NYC-WTC_000038451
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