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GCMS quantitation results for sample AE01548, March 2002

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Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.

NYC-WTC_000038414–000038419

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Dta File C:\MSDCHEM\l\DATA\022802\01548.D Vial: 24 Acq On 1 Mar 2002 7:25 am Operator: McLean • Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 13 06:45:06 2002 Quant Results File: 5080202.RES

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method SOSgcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.58 150 1114621 20.00 ug/L 0.00 10) Naphthalene-d8 13.05 136 2947996 20.00 ug/L 0.00 17) Acenaphthene-diO 18.16 164 1670053 20.00 ug/L 0.00 29) Phenanthrene-diO 22.52 188 2549649 20.00 ug/L 0.00 38) Chrysene-dl2 30.33 240 2389458 20.00 ug/L -0.03 44) Perylene-dl2 34.21 264 1522157 20.00 ug/L -0.02

System Monitoring Compounds 37) 2,4-ddd surr 27.46 235 199865 4.94 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.28 74 6895 0.20 ug/L 100 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1/3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 12 - Dichlorobenzene 0.00 146 0 N.D. 7) 22 ’ - oxybis (1-Chloropr 0.00 45 0 N.D. 8) NNitroso-di-n-propylamine 0.00 70 0 N.D. 9) Exachloroethane 0.00 117 0 N.D. 11) Nrobenzene 0.00 77 0 N.D. 12) Dphorone 0.00 82 0 N.D. 13) b; (2-Chloroethoxy) methan 0.00 93 _0 N.D. 14) 1,4-Trichlorobenzene 0.00 180 0 N.D. 15) Nhthalene 0.00 128 0 N.D. 16) Hichlorobutadiene 0.00 225 0 N.D. 18) Hefahlorocyclopentadiene —0.00 237 0 N.D. 19) 2 loronaphthalene / 0.00 162 0 N.D. 20) Dihylphthalate ( 0.00 163 0 N.D. 21) 2 Dinitrotoluene V 18.16 165 212445 9.14 ug/L # 25 22) ACphthylene 0.00 152 0 N.D. 23) ACohthene ) 0.00 153 0 N.D. 24) 2 nitrotoluene 0.00 165 0 N.D. 25) Dilphthalate 0.00 149 0 N.D. 26) 4 -rophenyl -phenyl ethe 0.00 204 0 N.D. 27) Flte 0.00 166 0 N.D. 28) AzQen/ 1,2 -DiphenyIhyd 0.00 77 0 N.D. 30) N-Nsodiphenylamine 0.00 169 0 N.D. 31) 4 -ohenyl -phenyl ether 0.00 248 0 N.D. 32) Hexrobenzene 0.00 284 0 N.D. 33) Phetrene 0.00 178 0 N.D. 34) Anthe 0.00 178 0 N.D. 35) Di-Ilphthalate 24.67 149 2722 0.02 ug/L 79 36) FluGene 0.00 202 0 N.D. 39) Pyre 0.00 202 0 N.D. 40) Butyylphthalate 0.00 149 0 N.D. 41) Benz antracene 0.00 228 0 N.D. d 42) Bis ylhexyl) phthala 30.94 149 82621 0.76 ug/L 96 43) Chryi 0.00 228 0 N.D. d 45) Di-Dhthalate 0.00 149 0 N.D. e 2 46) Benzluoranthene 0.00 252 0 N.D. #) = quabut of range (m) = manual integration 1548.D M Wed Mar 13 06:45:51 2002

NYC-WTC_000038416

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