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GCMS analysis results for sample AD31591, Feb 28 2002

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Laboratory report documenting GCMS analysis of sample AD31591 conducted on February 28, 2002.

NYC-WTC_000038205–000038219

Folder label: “GCMS X 2/21/02 A 2/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Dat'a File : C:\HPCHEM\1\DATA\JAN2502\31591.D Vial: 25 Acq On : 25 Jan 2002 2:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 27 15:11 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title - : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.83 178 969 N.D. 34) Anthracene 24.83 178 969 N.D. 35) Di-n-butylphthalate 26.78 149 12950 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.78 228 3574 N.D. 42) Bis(2-ethylhexyl)phthalate 33.09 149 6917 N.D. 43) Chrysene 32.78 228 3574 N.D. 45) Di-n-Octylphthalate 34.82 149 570 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 36.84 252 2959 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31591.D GCMS0208.M Wed Feb 27 15:12:02 2002 Page 2

NYC-WTC_000038218

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NYC-WTC_000038218Source: NYC Law Department, mirrored locally

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