GCMS analysis results for sample AD31587, Feb 28 2002

NYC 9/11 Public Portal Document

•$ LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\FEB2102\31587.D Vial: 34 Acq On : 22 Feb 2002 11:40 pm Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.199 340 344 359 rBV 100941 292280 13.16% 2.558% 2 12.330 789 794 808 rVB 644361 1605118 72.27% 14.049% 3 15.975 1185 1191 1208 rBV 1009929 2107938 94.90% 18.450% 4 21.290 1763 1770 1785 rBV 1039709 2221116 100.00% 19.440% 5 25.733 2247 2254 2266 rBV2 998420 2086834 93.95% 18.265%

6 25.880 2266 2270 2280 rVB2 7873 22848 1.03% 0.200% 7 30.810 2802 2807 2817 rVB 139890 269001 12. 11% 2.354% 8 33.803 3126 3133 3148 rBV2 688988 1603851 72.21% 14.038% 9 38.081 3590 3599 3619 rBV2 387058 1216403 54.77% 10.646%'

Sum of corrected areas: 11425389

31587.D GCMS0208.M Wed Feb 27 12:02:19 2002

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