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GCMS analytical results for sample AE03831, March 29, 2002

Machine-extracted title · confidence 100%

Laboratory report listing detection results for volatile organic compounds in sample AE03831 analyzed on March 29, 2002.

NYC-WTC_000038084–000038092

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

« Data File : C:\HPCHEM\1\DATA\MAR22O2\3831.D Vial: 12 Acq On : 23 Mar 2002 4:56 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.265 780 786 801 rVB 968735 2179662 68.12% 13.852% 2 14.863 1064 1069 1074 rBV 75500 140945 4.40% 0.896% 3 15.900 1176 1182 1199 rBV 1418538 2895643 90.50% 18.403% 4 21.206 1754 1760 1777 rBV 1504962 3199706 100.00% 20.335% 5 25.659 2238 2245 2256 rBV2 1439915 3113494 97.31% 19.787%

6 30.736 2792 2798 2806 rVB 211969 437075 13.66% 2.778% 7 33.719 3116 3123 3136 rBV2 1003520 2214971 69.22% 14.077% 8 37.970 3578 3586 3609 rBV2 525802 1553324 48.55% 9.872%

Sum of corrected areas: 15734820

3831 .D GCMS0308.M Tue Mar 26 14:59:18 2002

NYC-WTC_000038089

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NYC-WTC_000038089Source: NYC Law Department, mirrored locally

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