GCMS reference scan results for sample AE00364, March 21, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\031902\220REF2.D Vial: 7 Acq On : 19 Mar 2002 4:35 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 21 11:53:19 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.54 150 1912024 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 4871709 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.14 164 2721707 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.50 188 4263097 20.00 ug/L 0.00 38) Chrysene-dl2 30.32 240 3810366 20.00 ug/L 0.00 44) Perylene-dl2 34.19 264 2046267 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.43 235 386411 7.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 152.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.58 74 260616 6.07 ug/L 100 3) bis(2-chloroethyl) ether 8.98 93 771187 11.39 ug/L 81 4) 1,3 - Dichlorobenze 9.38 146 531850 7.95 ug/L 98 5) 1,4 - Dichlorobenzene 9.59 146 559653 8.38 ug/L 98 6) 1,2 - Dichlorobenzene 9.96 146 581603 9.41 ug/L 98 7) 2,2 ' - oxybis (l-Chloropr 10.43 45 1793978 11.64 ug/L 99 8) N-Nitroso-di-n-propylamine 10.76 70 629921 12.94 ug/L 95 9) Hexachloroethane 10.86 117 169620 6.76 ug/L 94 11) Nitrobenzene 11.10 77 802007 9.14 ug/L 97 12) Isophorone 11.81 82 1822611 11.29 ug/L 99 13) bis(2-Chloroethoxy) methan 12.55 93 949756 9.77 ug/L 100 14) 1,2,4-Trichlorobenzene 12.90 180 481453 8.63 ug/L 99 15) Naphthalene 13.08 128 2058024 10.16 ug/L 100 16) Hexachlorobutadiene 13.53 225 166825 5.35 ug/L 95 18) Hexachlorocyclopentadiene 15.61 237 77155 3.22 ug/L 100 19) 2-chloronaphthalene 16.51 162 1228040 9.88 ug/L 98 20) Dimethylphthalate 17.60 163 1682721 11.35 ug/L 98 21) 2,6-Dinitrotoluene 17.71 165 316854 10.04 ug/L 95 2 2) Acenaphthylene 17.70 152 1863353 10.81 ug/L 99 23) Acenaphthene 18.22 153 1247335 10.64 ug/L 100 24) 2,4-Dinitrotoluene 18.86 165 426033 9.43 ug/L 94 25) Diethylphthalate 19.73 149 1566108 12.27 ug/L 99 26) 4-Chlorophenyl-phenyl ethe 19.89 204 749367 11.02 ug/L 97 27) Fluorene 19.76 166 1629038 11.79 ug/L 100 28) Azobenzen/ 1,2-Diphenylhyd 20.35 77 1943606 10.33 ug/L 98 30) N-Nitrosodiphenylamine 20.26 169 847207 9.25 ug/L 98 31) 4-Bromophenyl-phenyl ether 21.32 248 436668 11.60 ug/L 92 32) Hexachlorobenzene 21.34 284 452932 11.41 ug/L 93 3 3) Phenanthrene 22.56 178 2285942 11.58 ug/L 99 34) Anthracene 22.70 178 2200925 11.23 ug/L 100 35) Di-n-butylphthalate 24.65 149 2720877 12.02 ug/L 99 36) Fluoranthene 26.06 202 2678155 11.94 ug/L 99 39) Pyrene 26.69 202 2751869 10.45 ug/L 99 40) Butylbenzylphthalate 29.05 149 1156013 10.25 ug/L 99 41) Benzo (a) antracene 30.29 228 2088992 10.45 ug/L 99 42) Bis (2-ethylhexyl) phthala 30.91 149 1512841 10.15 ug/L 96 43) Chrysene 30.39 228 2229952 11.74 ug/L 98 45) Di-n-Octylphthalate 32.75 149 2064439 9.39 ug/L 99 46) Benzo (b) fluoranthene 33.23 252 1629504 11.30 ug/L 99

(#) = qualifier out of range (m) = manual integration 220REF2.D 5080302.M Thu Mar 21 11:53:35 2002 Page 1

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