NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1401\29929.D Vial: 43
Acq On : 16 Dec 2001 - 7:44 am Operator: 209 GALOS
Sanpl e : gems scan 12/11 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 30 10:15 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Jan 25 15:57:52 2002
Response via : Initial Calibration
DataAcq Meth s GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 743315 20.00 ug/1 -0.03
10) Naphthalene-d8 15.28 136 2850069 20.00 ug/1 -0.03
17) Acenaphthene-dl0 20.55 164 1423722 20.00 ug/1 -0.03
29) Phenanthrene-diO 24.97 188 2013697 20.00 ug/1 -0.02
38) Chrysene-dl2 33.01 240 1233238 20.00 ug/1 -0.03
44) Perylene-dl2 37.10 264 770732 20.00 ug/1 -0.02
System Monitoring Compounds
37) 2,4-DDD 30.05 235 127710 5.77 ug/mL -0.02
Spiked Amount 5.000 Recovery = 115.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.16 74 2258 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’- oxybi s (1 - Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 13.01 77 173 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis (2 -Chloroethoxy) methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.34 128 1119 N.D.
16) Hexachiorobutadiene 0.00 225 0 N.D.
18) Hexachiorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 20.10 152 214 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.97 165 315 N.D.
25) Diethylphthalate 22.10 149 1314 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D,
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29929.D GCMS1126.M Wed Jan 30 10:16:55 2002 Page 1
NYC-WTC_000037475
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