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GCMS blank analysis results for sample AD29926, Jan 2002

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Blank quality control analysis for gas chromatography-mass spectrometry, completed January 30, 2002, measuring multiple semi-volatile organic compounds below method detection…

NYC-WTC_000037367–000037374

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1401\LBE.D Vial: 41 Acq On : 16 Dec 2001 5:47 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 30 9:57 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.65 168 562 N.D. 31) 4-Bromophenyl-phenylether 23.68 248 416 N.D. 32) Hexachlorobenzene 24.08 284 1285 N.D. 33) Phenanthrene 25.04 178 7524 N.D. 34) Anthracene 25.04 178 7524 N.D. 35) Di-n-butylphthalate 27.01 149 5762 N.D. 36) Fluoranthene 28.70 202 3764 N.D. 3 9) Pyrene 29.36 202 4317 N.D. 40) Butylbenzylphthalate 31.50 149 831 N.D. 41) Benzo(a)anthracene 33.01 228 7306 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 3226 N.D. 43) Chrysene 33.08 228 6436 N.D. 45) Di-n-Octylphthalate 35.04 149 2823 N.D. 46) Benzo(b)fluoranthene 36.12 252 5884 N.D. 47) Benzo(k)fluoranthene 36.12 252 2751 N.D. 48) Benzo(a)pyrene 36.94 252 1625 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.99 276 115 N.D.

(#) = qualifier out of range (m) = manual integration LBE.D GCMS1126.M Wed Jan 30 10:02:02 2002 Page 2

NYC-WTC_000037369

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NYC-WTC_000037369Source: NYC Law Department, mirrored locally

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