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GCMS analysis results for sample AD30016, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30016 conducted on January 28, 2002.

NYC-WTC_000037244–000037254

Folder label: “GCMS X 12/11/01 A 12/18/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\JAN1502\30016.D Vial: 25 Acq On : 15 Jan 2002 3:49 pm Operator: 209 GALOS Sample : gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 14:47 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue.

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.84 178 490 N.D. 3 4) Anthracene 24.84 178 490 N.D. 35) Di-n-butylphthalate 26.80 149 5375 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.81 228 5997 N.D. 42) Bis(2-ethylhexyl)phthalate 33.11 149 7003 N.D. 43) Chrysene 32.81 228 5997 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 35.88 252 172 N.D. 48) Benzo(a)pyrene 36.87 252 5654 N.D. 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g,h,i)perylene 0.00 276 0 N.D.

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(#) = qualifier out of range (m) = manual integration 30016.D GCMS1126.M Fri Jan 18 14:48:10 2002 Page 2

NYC-WTC_000037247

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NYC-WTC_000037247Source: NYC Law Department, mirrored locally

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Gas chromatography mass spectrometry report documenting analytical results for environmental samples processed in mid-February 2002.

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