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GCMS comments for sample AD29789 showing no unusual compounds, Jan

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Laboratory commentary noting a GCMS scan of sample AD29789 revealed no unusual compounds on January 9, 2002.

NYC-WTC_000037135–000037145

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1401\29789.D Vial: 21 Acq On : 15 Dec 2001 10:02 pm Operator: 209 GALOS Sample : gcms scan 12/10 a Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 22:50 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.06 178 460 N.D. 34) Anthracene 25.06 178 460 N.D. 35) Di-n-butylphthalate 26.99 149 10892 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.51 149 365 N.D. 41) Benzo(a)anthracene 33.01 228 3951 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 11962 N.D. 43) Chrysene 33.01 228 3951 N.D. 45) Di-n-Octylphthalate 35.04 149 691 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.10 252 3946 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene .0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 29789.D GCMS1126.M Fri Dec 28 12:54:07 2001 Page. 2

NYC-WTC 000037138

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NYC-WTC_000037138Source: NYC Law Department, mirrored locally

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