Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
NYC-WTC_000036614–000036644Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: junk · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
' Data File C:\HPCHEM\1\DATA\JANO 02\2 94 6 6.D Vial: 6 Acq On 8 Jan 2002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\l\METHCDS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer Baseline drop else tangent Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 6.993 207 212 227 rBV 114654 339616 2.21% 0.183% 2 7.479 260 265 280 rBV3 395204 1400996 9.11% 0.756% 3 9.306 458 464 479 rBV2 36006 171535 1.12% 0.093% 4 10.518 592 596 598 rBV 85476 176353 1.15% 0.095% 5 10.554 598 600 606 rW3 74909 244769 1.59% 0.132%
6 10.995 642 648 662 rBV 1575934 3893495 25.32% 2.101% 7 11.197 662 670 675 rW 302162 748672 4.87% 0.404% 8 11.280 675 679 • 683 rW 283242 636750 4.14% 0.344% 9 11.353 683 687 692 rW 107838 312429 2.03% 0.169% 10 11.436 692 696 699 rW2 194496 474719 3.09% 0.256%
11 11.528 699 70 6 715 rW2 2964927 8371948 54.43% 4.519% 12 11.665 715 721 729 rVB 402826 1193657 7.76% 0.644% 13 11.821 734 738 745 rBV 121726 278782 1.81% 0.150% 14 11.941 745 751 755 rBV 291812 650416 4.23% 0.351% 15 12.005 755 758 766 rVB 110193 294086 1.91% 0.159%
16 12.124 766 771 779 rVB4 51420 169608 1.10% 0.092% 17 12.253 779 785 788 rBV3 65667 183927 1.20% 0.099% 18 12.363 788 797 801 rBV2 496275 1651147 10.74% 0.891% 19 12.519 809 814 818 rBV 490275 1095574 7.12% 0.591% 20 12.629 823 826 831 rVB2 88259 195489 1.27% 0.106%
21 12.804 839 845 854 rW3 380400 1458795 9.49% 0.787% 22 12.932 854 859 864 rW2 151049 388886 2.53% 0.210% 23 13.015 865 868 871 rW2 89555 233076 1.52% 0.126% 24 13.070 871 874 880 rVB2 102360 239956 1.56% 0.130% 25 13.235 888 892 895 rW 106508 319348 2.08% 0.172%
26 13.281 895 897 900 rW 117429 253137 1.65% 0.137% 27 13.630 931 935 941 rW 204139 604329 3.93% 0.326% 28 13.722 941 945 94 9 rW 594077 1229716 8.00% 0.664%
NYC-WTC_000036620
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NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036492
Fragmented page from a DEP environmental sampling record containing partial text and data fields.
Filed in the same folder
NYC-WTC_000036494
Laboratory calibration data sheet for GCMS analysis of organic compounds including nitrosamines and chlorobenzenes dated December 13, 2001.
Filed in the same folder
NYC-WTC_000036498
Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
Filed in the same folder
NYC-WTC_000036503
Laboratory report documenting GCMS blank analysis for organic compounds conducted on January 4, 2002, showing results below detection limits.
Filed in the same folder