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GCMS sample analysis AD29291, Dec 2001

Machine-extracted title · confidence 95%

Laboratory analysis report for sample AD29291 conducted on December 28, 2001, including surrogate recovery data.

NYC-WTC_000036232–000036242

Folder label: “GCMS X 12/4/01 A 12/10/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

ta File : C:\HPCHEM\1\DATA\DEC1001\29235.D Vial: 8 G On : 12 Dec 2001 6:34 am Operator: 209 GALOS ample : gc/ms scan 12/4 Inst : GC/MS 209 isc Multiplr: 1.00 S Integration Params: LSCINT.P

ethod : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) 'itle : 209 625/TCLP calibration table moothing : OFF Filtering: 5 Jampling : 1 Min Area: 1 % of largest Peak tart Thrs: 0.2 Max Peaks: 100 >top Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

eak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 309 rBV 329226 1030334 14.72% 2.882% 2 11.348 683 687 692 rBV 78314 183997 2.63% 0.515% 3 11.431 692 696 715 rVB 81854 269635 3.85% 0.754% 4 11.670 715 722 745 rBV 1894119 5114626 73.06% 14.306% 5 15.277 1109 1115 1133 rBV 2886304 6331790 90.45% 17.710%

6 20.547 1683 1689 1711 rBV 3136165 7000548 100.00% 19.581% 7 24.972 2164 2171 2183 rBV2 2849001 6256330 89.37% 17.499% 8 25.119 2184 2187 2198 rVB2 24542 79646 1.14% 0.223% 9 30.049 2718 2724 2731 rBV 472046 954783 13.64% 2.671% 10 33.005 3039 3046 3064 rBV2 1988880 4658009 66.54% 13.029%

11 37.099 3484 3492 3509 rBV 1362569 3872131 55.31% 10.831%

Sum of corrected areas: 35751829

29235.D GCMS1126.M Wed Dec 19 12:52:37 2001

NYC-WTC_000036237

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NYC-WTC_000036237Source: NYC Law Department, mirrored locally

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