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GCMS analysis comments, sample AD29230, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.

NYC-WTC_000036114–000036125

Folder label: “GCMS X 12/3/01 A 12/10/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C: \HPCHEM\ 1 \DATA\DEC10 01\29230.D Vial: 18 Acq On : 11 Dec 2001 3:18 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 15:28 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 1112 N.D. 3 4) Anthracene 25.04 178 1112 N.D. 35) Di-n-butylphthalate 26.99 149 33345 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.01 228 3308 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 19572 N.D. 43) Chrysene 33.01 228 3308 N.D. 45) Di-n-Octylphthalate 34.61 149 166 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.10 252 3880 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29230.D GCMS1126.M Fri Dec 14 15:38:14 2001 Page 2

NYC-WTC_000036117

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NYC-WTC_000036117Source: NYC Law Department, mirrored locally

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