Laboratory report noting detection of Decanedioic acid bis(2-Ethylhexyl) ester in sample AD29027 on December 18, 2001.
NYC-WTC_000035931–000035943Folder label: “GCMS X 11/30/01 A 12/11/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC1001\29027.D Vial: 28 Acq On : 11 Dec 2001 3:01 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise : Multiplr: 1.. 00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:38 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1097694 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 4133050 20.00 ug/1 -0.02 17) Acenaphthene-dlO 20.55 164 2078080 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3015633 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1996132 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1366653 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 154912 4.31 ug/mL -0.02 .Spiked Amount 5.000 Recovery = 86.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.26 74 110 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.14 77 111 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1282 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.18 165 294 N.D. 25) Diethylphthalate 22.08 149 1321 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 29027.D NP091101.M Mon Dec 17 13:15:31 2001 Page 1
NYC-WTC_000035933
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NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036391
Laboratory report documenting GCMS analysis of sample AD29298 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037314
Gas chromatography-mass spectrometry report documenting analysis of sample AD30011 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037301
Gas chromatography-mass spectrometry report documenting analysis of sample AD30014 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036311
Laboratory analysis report for sample AD29285 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.997
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NYC-WTC_000035888
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035889
Fragmented laboratory data sheet recording sample volumes and drip rates for GCMS Method S08 analysis.
Filed in the same folder
NYC-WTC_000035890
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
Filed in the same folder
NYC-WTC_000035900
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035904
Document containing reference values and recovery data for organic compounds analyzed by GCMS.
Filed in the same folder