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GCMS analysis results, sample AD28903, Dec 2001

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GCMS analysis results for sample AD28903 dated December 15, 2001, showing non-detect levels for various compounds.

NYC-WTC_000035563–000035570

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 7 01\LB.D Vial: 7 Acq On 7 Dec 2001 8:47 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 312 rBV 535145 1318910 17.46% 3.415% 2 11.670 717 722 741 rBV 2232439 5227059 69.18% 13.534% 3 15.278 1109 1115 1134 rBV 3271445 6926335 91.67% 17.934% 4 20.556 1683 1690 1708 rBV 3458115 7555622 100.00% 19.564% 5 24.972 2165 2171 2184 rBV2 3031235 7048682 93.29% 18.251%

6 25.119 2184 2187 2202 rVB2 27054 91873 1.22% 0.238% 7 30.049 2719 2724 2731 rBV 483955 1000303 13.24% 2.590% 8 33.014 3037 3047 3061 rBV 2189113 5126835 67.85% 13.275% 9 33.289 3072 3077 3086 rVB 61617 146875 1.94% 0.380% 10 37.099 3485 3492 3505 rBV2 1474164 4177871 55.29% 10.818%

Sum of corrected areas: 38620365

LB.D GCMS1126.M Thu Dec 13 10:31:24 2001

NYC-WTC_000035567

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NYC-WTC_000035567Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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