GCMS analysis results, sample AD28323, Jan 2002

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GCMS analysis results for sample AD28323 dated January 3, 2002, showing surrogate compound results.

NYC-WTC_000035540–000035549

Folder label: “GCMS X 11/28/01 A 12/28/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC2801\28323.D Vial: 8 Acq On : 28 Dec 2001 2:17 pm Operator: GALOS Sample : gems unknown 11/28 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 3 12:27 2002 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.84 152 761677 20.00 ng/uL -0.10 19) Naphthalene-d8 15.44 136 3057790 20.00 ng/uL -0.11 31) Acenaphthene-diO 20.71 164 1367262 2 0.00 ng/uL -0.11 49) Phenanthrene-diO 25.12 188 1971795 20.00 ng/uL -0.12 59) Chrysene-dl2 33.13 240 1380871 2 0.00 ng/uL -0.12 68) Perylene-dl2 37.21 264 876660 2 0.00 ng/uL -0.13

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.84 132 302 0.01 ng/uL 0.41 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 11.97 152 303 0.01 ng/uL -0.48 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 0.00 172 0 0.00 ng/uL Spiked Amount 50.000 Range 42 78 Recovery = 0.00%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 3) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration 28323.D NP112701.M Thu Jan 03 12:27:25 2002 Page 1

NYC-WTC_000035542

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