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GCMS analysis comments, sample AD28859, December 2001

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Gas chromatography-mass spectrometry analysis results for sample AD28859 showing bis(2-Ethylhexyl)phthalate presence at 0.81 ug/L with quality control notes on LCS standard recover

NYC-WTC_000035505–000035513

Folder label: “GCMS X 11/27/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC0601\28859.D Vial: 31 Acq On 7 Dec 2001 4:57 am Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 5:46 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 0.00 162 0 N.D. 31) Dimethylphthalate 19.93 163 290 N.D. 32) 2,6-Diriitrotoluene 20.11 165 187 N.D. 33) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.23 65 186 N.D. 37) 2,4-Dinitrotoluene 21.16 165 218 N.D. 38) Diethylphthalate 22.07 149 4485 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 23.07 77 288 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 25.03 178 1024 N.D. 49) Anthracene 25.03 178 1024 N.D. 50) Di-n-butylphthalate 26.99 149 42211 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.50 149 738 N.D. 56) Benzo(a)anthracene 33.00 228 5049 N.D. 57) Bis(2-ethylhexyl)phthalate 33.29 149 90102 0.81 ug/1 97 58) Chrysene 33.00 228 5049 N.D. 60) Di-n-Octylphthalate 35.04 149 3114 N.D. 61) Benzo(b)fluoranthene 0.00 252 0 N.D. 62) Benzo(k)fluoranthene 0.00 252 0 N.D. 63) Benzo(a)pyrene 37.10 252 4998 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28859.D GCMS1126.M Tue Dec 11 12:12:02 2001 Page 2

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