GCMS scan results for sample AD28802 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate and other compounds.
NYC-WTC_000035460–000035472Folder label: “GCMS X 11/27/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\DEC0601\28802.D Vial: 29 Acq On 7 Dec 2001 3:00 am Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 3:48 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP. calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1085140 20.00 ug/1 -0.03 15) Naphthalene-d8 15.28 136 4090048 20.00 ug/1 -0.03 26) Acenaphthene-dlO 20.56 164 2029854 20.00 ug/1 -0.02 42) Phenanthrene-dlO 24.97 188 2976527 20.00 ug/1 -0.02 53) Chrysene-dl2 33.01 240 1920177 20.00 ug/1 -0.03 59) Perylene-dl2 37.10 264 1370905 20.00 ug/1 -0.02
System Monitoring Compounds 52) 2,4-DDD 30.05 235 196426 5.54 ug/mL -0.02 Spiked Amount 5.000 Recovery = 110.80%
Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.25 74 867 N.D. 4) Phenol 11.01 94 351 N.D. 5) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 6) 2-Chlorophenol 0.00 128 0 N.D. 7) 1,3-Dichlorobenzene 0.00 146 0 N.D. 8) 1,4-Dichlorobenzene 0.00 146 0 N.D. 9) 1,2-Dichlorobenzene 0.00 146 0 N.D. 10) 2-Methylphenol 0.00 108 0 N.D. 11) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 12) 3&4-Methylphenol 0.00 108 0 N.D. 13) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 14) Hexachloroethane 0.00 117 0 N.D. 16) Nitrobenzene 12.93 77 2699 N.D. 17) Isophorone 14.04 82 496 N.D. 18) 2-Nitrophenol 0.00 139 0 N.D. 19) 2,4-Dimethylphenol 0.00 107 0 N.D. 20) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 21) 2,4-Dichlorophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 23) Naphthalene 15.33 128 2260 N.D. 24) Hexachlorobutadiene 0.00 225 0 N.D. 25) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 27) Hexachlorocyclopentadiene 0.00 237 0 N.D. 28) 2,4,6-Trichlorophenol 0.00 196 0 N.D.
(#) = qualifier out of range (m) = manual integration 28802.D GCMS1126.M Tue Dec 11 15:39:08 2001 Page 1
NYC-WTC_000035462
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NYC-WTC_000036311
Laboratory analysis report for sample AD29285 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035640
Lab report noting bis(2-Ethylhexyl)phthalate detection, recovery issues, and low pH.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036137
Laboratory report noting GCMS scan results for sample AD29233 with phthalates and nonadecanol detected.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035618
Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036391
Laboratory report documenting GCMS analysis of sample AD29298 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033580
Laboratory report documenting GCMS analysis of environmental sample AD27771 conducted on January 3, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033674
Gas chromatography-mass spectrometry analysis of environmental sample AD27826 conducted on January 3, 2002, detecting unknown compounds and 2,4-DDD surrogate standard.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032160
Laboratory report documenting GCMS analysis of sample AD26827 identifying unknown compounds on December 21, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000035422
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035423
Label for a GCMS environmental sample collected between November and December 2001.
Filed in the same folder
NYC-WTC_000035426
Log recording sample volume, drip rates, and addition details for GCMS analysis in December 2001.
Filed in the same folder
NYC-WTC_000035435
Laboratory report of a method blank analyzed on December 16, 2001, showing non-detect results for target compounds.
Filed in the same folder
NYC-WTC_000035439
Calibration data for GCMS analysis of volatile organic compounds dated December 6, 2001.
Filed in the same folder