GCMS analysis report, Jan 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

•..Data File : C:\HPCHEM\1\DATA\DEC2101\28309.D Vial: 41 Acq On : 22 Dec 2001 5:37 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 28 9:02 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.79 152 827733 20.00 ng/uL -0.15 19) Naphthalene-d8 15.39 136 3335164 20.00 ng/uL -0.16 31) Acenaphthene-diO 20.67 164 1477445 20.00 ng/uL -0.16 49) Phenanthrene-dlO 25.08 188 2210634 20.00 ng/uL -0.17 59) Chrysene-dl2 33.08 240 1532318 20.00 ng/uL -0.17 68) Perylene-dl2 37.15 264 965579 20.00 ng/uL -0.18

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.78 132 596 0.01 ng/uL 0.36 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 0.00 152 0 0.00 ng/uL Spiked Amount 50.000 Range 26 73 Recovery = 0.00%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.81 172 1522 0.02 ng/uL -0.02 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue . 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 '108 0 N.D. 15) 2,21 -oxybis(l-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration 28309.D NP112701.M Fri Dec 28 09:05:50 2001 Page 1

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