GCMS analysis comments for sample AD28677, Dec 2001

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0401\28677.D Vial: 13 Acq On 5 Dec 2001 12:05 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.707 721 726 747 rBV 1971227 5006285 73.64% 12.890% 2 15.314 1113 1119 1137 rBV 3099066 6547868 96.32% 16.859% 3 20.584 1687 1693 1713 rBV 3049771 6798314 100.00% 17.504% 4 25.009 2168 2175 2187 rBV2 2791400 6188744 91.03% 15.934% 5 25.156 2187 2191 2201 rVB2 25656 85281 1.25% 0.220%

6 29.434 2652 2657 2665 rBV 806598 1598142 23.51% 4.115% 7 29.553 2665 2670 2677 rW 102607 211568 3.11% 0.545% 8 29.682 2679 2684 2696 rVB 92608 198168 2.91% 0.510% 9 30.076 2721 2727 2734 rBV 225245 441528 6.49% 1.137%. 10 30.627 2782 2787 2795 rBV 94066 194554 2.86% 0.501%

11 31.573 2884 2890 2896 rBV 515863 1068961 15.72% 2.752% 12 31.665 2896 2900 2910 rW 146869 338679 4.98% 0.872% 13 31.793 2910 2914 2926 rVB2 27645 75055 1.10% 0.193% 14 32.656 3002 3008 3016 rBV 110973 239005 3.52% 0.615% 15 33.032 3041 3049 3061 rBV2 1843318 4360313 64.14% 11.226%

16 33.611 3106 3112 3124 rBV 114225 270374 3.98% 0.696% 17 34.538 3206 3213 3223 rBV 72905 186732 2.75% 0.481% 18 35.428 3304 3310 3321 rBV 52247 143579 2.11% 0.370% 19 36.282 3398 3403 3417 rVB2 27725 84439 1.24% 0.217% 20 36.723 3445 3451 3460 rBV 38501 127510 1.88% 0.328%

21 37.127 3488 3495 3513 rBV2 1174109 3455596 50.83% 8.897% 22 38.036 3585 3594 3603 rBV2 43518 180059 2.65% 0.464% 23 39.596 3757 3764 3781 rBV5 42701 225971 3.32% 0.582% 24 41.561 3965 3978 3988 rBV5 46239 289855 4.26% 0.746% 25 43.975 4227 4241 4254 rBV4 36833 292536 4.30% 0.753%

26 47.051 4563 4576 4597 rBV7 25699 230570 3.39% 0.594%

NYC-WTC_000035175