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GCMS analysis comments for sample AD28691, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28691.

NYC-WTC_000035052–000035071

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary Operator ID: 209 GALOS Date Acquired: 4 Dec 2001 10:08 pm Data File: C:\HPCHEM\1\DATA\DEC0401\28691.D Name: gc/ms 11/24 Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

1-Butanamine, 3 -meth 7.66 0.4 ug/1 95862 ISTD01 11.71 4560120 20.0 Cyelobutane, 1,1- dim 29.44 9.3 ug/1 2123230 ISTD05 33.04 4558130 20.0 Docosane 29.56 1.2 ug/1 265911 ISTD05 33.04 4558130 20.0 l-Heptadecanol, acet 29.68 1.2 ug/1 270660 ISTD05 33.04 4558130 20.0 Tricosane 3 0.63 1.1 ug/1 253767 ISTD05 33.04 4558130 20.0 Octade eancic acid, 2 31.58 6.6 ug/1 1492880 ISTD05 33.04 4558130 20.0 Tetracosane 31.67 1.9 ug/1 441012 ISTD05 33.04 4558130 20.0 Acetic acid, octadec 31.80 0.5 ug/1 107718 ISTD05 33.04 4558130 20.0 Hexatriacontane 32.66 1.4 ug/1 325553 ISTD05 33.04 4558130 20.0 Hexadecane 33.61 1.7 ug/1 387370 ISTD05 33.04 4558130 20.0 Hexatriacontane 34.53 1.1 ug/1 247833 ISTD05 33.04 4558130 20.0 Pentacosane 35.42 1.1 ug/1 212422 ISTD06 37.13 3810050 20.0 Heptadecane 36.29 0.6 ug/1 115981 ISTD06 37.13 3810050 20.0

28691.D GCMS1126.M Thu Dec 06 13:26:57 2001

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NYC-WTC_000035071

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NYC-WTC_000035071Source: NYC Law Department, mirrored locally

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