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GCMS analysis comments for sample AD28662, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.

NYC-WTC_000034988–000034999

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2601\28680.D Vial: 11 Acq On : 28 Nov 2001 3:03 am Operator: 209 GALOS Sample : 11/24 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 6 13:16 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 33) Acenaphthylene 0.00 152 0 N.D. 34) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.03 165 112 N.D. 38) Diethylphthalate 22.10 149 321 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.00 178 521 N.D. 49) Anthracene 25.00 178 521 N.D. 50) Di-n-butylphthalate 27.01 149 10834 N.D. 51) Fluoranthene 0.00 202 0 N.D. ' 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 0.00 149 0 N.D. 56) Benzo(a)anthracene 33.02 228 2131 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 14449 0.29 ug/1 99 58) Chrysene 33.02 228 2131 N.D. 60) Di-n-Octylphthalate 35.03 149 208 N.D. 61) Benzo(b)fluoranthene 36.07 252 181 N.D. 62) Benzo(k)fluoranthene 36.12 252 465 N.D. 63) Benzo(a)pyrene 37.12 252 2207 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28680.D GCMS1126.M Thu Dec 06 13:17:07 2001 Page 2

NYC-WTC_000034990

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NYC-WTC_000034990Source: NYC Law Department, mirrored locally

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