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← Document results/DEP Box 22/GCMS X 11/23/01 A 11/29/01
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GCMS comments for sample AD28665, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28665 analyzed in early December 2001.

NYC-WTC_000034844–000034851

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2901\28665.D Vial: 42 Acq On : 30 Nov 2001 3:16 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.565 706 710 719 rBV 46361 113115 1.90% 0.401% 2 11.694 719 724 743 rBV 1642691 4347341 73.11% 15.413% 3 15.301 1111 1117 1135 rBV 2736294 5787926 97.34% 20.520% 4 20.571 1685 1691 1713 rBV 2722856 5946205 100.00% 21.082% 5 24.996 2166 2173 2187 IBV2 2402711 5225733 87.88% 18.527%

6 30.072 2720 2726 2736 rBV 269897 555931 9.35% 1.971% 7 33.029 3041 3048 3066 rBV2 1481005 3541997 59.57% 12.558% 8 37.114 3485 3493 3509 rBV2 963512 2687374 45.19% 9.528%

Sum of corrected areas: 28205622

28665.D GCMS1126.M Fri Nov 30 16:20:29 2001

NYC-WTC_000034848

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NYC-WTC_000034848Source: NYC Law Department, mirrored locally

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