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Document / 9 pages

GCMS comments for sample AD28652, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28652 analyzed in early December 2001.

NYC-WTC_000034781–000034789

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV2901\28595.D Vial: 37 Acq On : 29 NOV 2001 10:23 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 7.760 292 296 311 rBV2 38302 150853 2.44% 0.537% 2 11.561 706 710 720 rBV 48278 116635 1.89% 0.416% 3 11.698 720 725 751 rVB 1739874 4592203 74.40% 16.360% 4 15.297 1112 1117 1136 rBV 2748593 6057291 98.14% 21.580% 5 20.576 1685 1692 1710 rBV 2845159 6172370 100.00% 21.990% 6 24.991 2167 2173 2186 rBV2 2453407 5225758 84.66% 18.618% 7 30.068 2720 2726 2733 rVB 244829 482134 7.81% 1.718% 8 33.024 3041 3048 3064 rBV2 1326168 3094913 50.14% 11.026% 9 37.109 3486 3493 3511 rBV 799130 2176897 35.27% 7.756%

Sum of corrected areas: 28069054 28595.D GCMS1126.M Fri Nov 30 15:29:04 2001

NYC-WTC_000034785

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NYC-WTC_000034785Source: NYC Law Department, mirrored locally

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