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Document / 9 pages

GCMS comments for sample AD28594, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results detecting bis(2-ethylhexyl)phthalate and recovery rates for sample AD28594.

NYC-WTC_000034750–000034758

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C: \HPCHEM\ 1 \DATA\NOV2 901\28600.D Vial: 39 Acq On : 30 NOV 2001 12:20 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.621 277 281 302 rBV 349655 1019564 16.08% 3.322% 2 11.560 706 710 720 rBV 46809 120551 1.90% 0.393% 3 11.697 720 725 744 rBV 1825773 4603622 72.61% 14.999% 4 15.305 1112 1118 1136 rBV 2736735 6118743 96.51% 19.935% 5 20.575 1685 1692 1715 rBV 2890768 6339922 100.00% 20.656%

6 24.990 2167 2173 2187 rBV2 2521393 5589676 88.17% 18.212% 7 30.067 2721 2726 2735 rW 334456 661284 10.43% 2.155% 8 33.023 3041 3048 3066 rBV2 1619160 3651703 57.60% 11.897% 9 37.118 3486 3494 3510 rBV2 909035 2587965 40.82% 8.432%

Sum of corrected areas: 30693030 28600.D GCMS1126.M Fri Nov 30 14:49:49 2001

NYC-WTC_000034754

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NYC-WTC_000034754Source: NYC Law Department, mirrored locally

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