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GCMS analysis results for sample AD28468, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD28468 conducted between November 21 and 26, 2001.

NYC-WTC_000034366–000034374

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\28468.D Vial: 24 Acq On : 29 Nov 2001 10:39 am Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 15:24 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 867731 20.00 ug/1 0.00 15) Naphthalene-d8 15.30 136 3274455 20.00 ug/1 -0.01 26) Acenaphthene-diO 20.57 164 1542443 20.00 ug/1 0.00 42) Phenanthrene-diO 24.99 188 2074595 20.00 ug/1 0.00 53) Chrysene-dl2 33.02 240 918703 20.00 ug/1 -0.01 59) Perylene-dl2 37.11 264 545915 20.00 ug/1 -0.01 System Monitoring Compounds 52) 2,4-DDD 30.07 235 94179 3.81 ug/mL 0.00 Spiked Amount 5.000 Recovery = 76.20% Target Compounds Qvalue 2) Pyridine 5.25 79 N.D. 3) N-nitroso-dimethyl amine 0.00 74 N.D. 4) Phenol 11.06 94 198 N.D. 5) bis(2-Chloroethyl)ether 6) 2-Chlorophenol 7) 1,3-Dichlorobenzene 11.16 0.00 11.73 93 128 146 829 N.D. N.D. N.D. 8) 1,4-Dichlorobenzene 11.73 146 (235 N.D. 9) 1,2-Dichlorobenzene 0.00 146 235) N.D. 10) 2-Methylphenol 11) 2,2' -oxybis(1-Chloropropan 12) 3&4-Methylphenol 12.40 0.00 0.00 108 45 108 S1 0 N.D. N.D. N.D. 13) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 14) Hexachloroethane 0.00 117 —0 N.D. 16) Nitrobenzene 13.47 77 ( ' 18 3 N.D. 17) Isophorone 14.07 82 1082 N.D. 18) 2-Nitrophenol 0.00 139 N.D. 19) 2,4-Dimethylphenol 0.00 107 0 N.D. 20) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 21) 2,4-Dichlorophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 15.20 180 197 N.D. 23) Naphthalene 15.36 128 2041 " N.D. 24) Hexachlorobutadiene 0.00 225 0 N.D. 25) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 27) Hexachlorocyclopentadiene 0.00 237 0 N.D. 28) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 18.86 162 608 N.D. 31) Dimethylphthalate 19.96 163 1079 N.D. 32) 2,6-Dinitrotoluene 0.00 165 0 N.D. d (#) = qualifier out of range (m) = manual integration 28468.D GCMS1126.M Thu Nov 29 15:24:52 2001 Page 1

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