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Document / 9 pages

GCMS analysis results for sample AD28277, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28277 conducted between November 21 and 26, 2001.

NYC-WTC_000034249–000034257

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM \1\DATA\NOV2 601\28277.D Vial: 28 Acq On : 27 NOV 2001 3:19 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks; 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.558 706 710 720 rBV 44847 118289 2.00% 0.445% 2 11.696 720 725 745 rBV 1697438 4380732 74.06% 16.487% 3 15.304 1112 1118 1135 rBV 2662663 5804668 98.13% 21.846% 4 20.574 1686 1692 1708 rBV 2871700 5915266 100.00% 22.262% 5 24.998 2167 2174 2187 rBV2 2321693 5090430 86.06% 19.158%

6 30.075 2721 2727 2737 rBV 143897 296110 5.01% 1.114% 7 33.022 3042 3048 3068 rBV2 1202917 2857478 48.31% 10.754% 8 37.116 3487 3494 3510 rBV2 767377 2108413 35.64% 7.935%

Sum of corrected areas: 26571386 28277.D GCMS1126.M Fri Nov 30 13:22:47 2001

NYC-WTC_000034254

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NYC-WTC_000034254Source: NYC Law Department, mirrored locally

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