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GCMS unknowns analysis results for sample AD28335, Jan 2002

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Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.

NYC-WTC_000033974–000034002

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\JAN0802\28335A.D Vial: 4 Acq On 8 Jan 2002 6:13 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 9:04 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 / N.D. 3 3) Phenanthrene 24.81 178 2038 4 N.D. 34) Anthracene 24.81 178 2038 ' N.D. 35) Di-n-butylphthalate 26.83 149 19465 / N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0/ N.D. d 41) Benzo(a)anthracene 32.84 228 4402 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 3127 / N.D. 43) Chrysene 32.84 228 4402 N.D. 45) Di-n-Octylphthalate 0.00 149 0 / N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. s 48) Benzo(a)pyrene 36.91 252 4506 N.D. 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28335A.D GCMS1126.M Wed Jan 09 09:57:14 2002 Page 2

NYC-WTC_000033977

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NYC-WTC_000033977Source: NYC Law Department, mirrored locally

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