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GCMS unknowns analysis results for sample AD28326, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28326 conducted on January 9, 2002.

NYC-WTC_000033945–000033953

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV2 601\28326.D Vial: 17 Acq On : 28 Nov 2001 9:54 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.64 0 279 283 294 rBV 26370 78051 1.08% 0.242% 2 11.560 705 710 719 rVB 60277 140029 1.94% 0.434% 3 11.698 719 725 742 rBV 2199876 5394438 74.73% 16.700% 4 15.305 1111 1118 1136 rBV 3174982 7076063 98.03% 21.906% 5 20.575 1685 1692 1717 rBV 3347038 7218350 100.00% 22.347%

6 24.991 2167 2173 2186 rBV2 2688075 6045823 83.76% 18.717% 7 30.067 2721 2726 2731 rBV 273569 548063 7.59% 1.697% 8 33.023 3041 3048 3063 rBV2 1494069 3366883 46.64% 10.423% 9 37.118 3486 3494 3508 rBV 885053 2433597 33.71% 7.534%.,

Sum of corrected areas: 32301297

28326.D GCMS1126.M Thu Jan 03 12:48:50 2002

NYC-WTC_000033950

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NYC-WTC_000033950Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28265, Nov 2001 · Box DEP Box 21

NYC-WTC_000033825

Analytical commentary for sample AD28265 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗
GCMS comments for sample AD28149, Nov 2001 · Box DEP Box 21

NYC-WTC_000033780

Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗

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