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GCMS analysis comments for sample AD28147, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting the presence of bis(2-Ethylhexyl)phthalate and recovery rates for environmental sample AD28147 analyzed in December 2001.

NYC-WTC_000033884–000033885

Folder label: “GCMS X 11/20/01 A 11/26/01

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Scanned page image, NYC-WTC_000033885
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

DFTPP

Data File M:\INSTRU-1\2 09\DATA\NOV2601\DFTPP.D Vial: 1 Acq On 26 Nov 2001 10:40 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D

5000000

4000000

3000000

; 2000000

1000000

, 41 0+ 24'40 24.60 24'80 T / +_ I IP T_A_ ।___ !___ PIIITI Time-> 25.00 25'20 25'40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00___ Abundance ".. ’ ’ Average of 26.224 to 26.251 min.: DFTPP.D 198 500000

400000 442 300000 127 255 69 200000 51 110 275 100000 224

1miz- > 0 31 L.481671d 38 +1rer 1H—H* ■ ■ i ■ ■ 40 60 93 L 296 211.248 ,1L — „ 216310323336,852325.883. 403.423. , ,41122 i 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 80 423

Spectrum Information: Average of 26.224 to 26.251 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 30.8 175908 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 40.5 231312 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 44.7 254976 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 570816 PASS 199 198 5 9 6.6 37502 PASS 275 198 10 30 20.3 115872 PASS 365 198 1 100 1.8 10464 PASS 441 443 0.01 100 92.0 54000 PASS 442 198 40 110 53.7 306592 PASS 443 442 17 23 19.1 58668 PASS

DFTPP.D GCMS1126.M Wed Jan 09 14:19:11 2002

NYC-WTC_000033885

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NYC-WTC_000033885Source: NYC Law Department, mirrored locally

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