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GCMS analysis results for sample AD27546, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD27546 for unknown compounds and surrogates on December 18, 2001.

NYC-WTC_000033448–000033457

Folder label: “GCMS X 11/15/01 A 12/13/01

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Scanned page image, NYC-WTC_000033454
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27546.D Vial: 5 Acq On 13 Dec 2001 2:01 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.822 322 325 341 rBV 390191 860395 8.90% 1.779% 2 11.866 760 766 782 rBV 3624108 7445640 77 ..04% 15.395% 3 15.470 1153 1159 1177 rBV 4940184 9664775 100.00% 19.983% 4 20.742 1728 1734 1751 rBV 4652941 9373874 96.99% 19.382% 5 25.153 2208 2215 2226 rBV2 4274733 8895717 92.04% 18.393%

6 33.150 3080 3087 3102 rBV2 2962203 6735704 69.69% 13.927% 7 37.239 3524 3533 3553 rBV2 2008383 5388152 55.75% 11.141%

Sum of corrected areas: 48364257

27546.D NP112701.M Fri Dec 14 12:54:49 2001

NYC-WTC_000033454

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NYC-WTC_000033454Source: NYC Law Department, mirrored locally

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