GCMS analysis results for sample AD27765, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1901\27765.D Vial: 8 Acq On : 20 Dec 2001 2:18 am Operator : GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 11:14 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.87 152 725600 20.00 ng/uL -0.06 19) Naphthalene-d8 15.49 136 2814542 20.00 ng/uL -0.06 31) Acenaphthene-dlO 20.76 164 1249238 2 0.00 ng/uL -0.06 49) Phenanthrene-dlO 25.17 188 1827363m 20.00 ng/uL -0.07 59) Chrysene-dl2 33.18 240 1148618 20.00 ng/uL -0.07 68) Perylene-dl2 37.26 264 529550 20.00 ng/uL -0.08

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.87 132 314 0.01 ng/uL 0.45 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 11.98 152 673 0.02 ng/uL -0.48 Spiked Amount 50.000 Range 26 73 Recovery = 0.04%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.91 172 1622 0.02 ng/uL 0.08 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 30.05 244 2083 0.04 ng/uL -0.08 Spiked Amount 50.000 Range 58 98 Recovery . = 0.08%#

Target Compounds Qvalue 2) Pyridine 5.50 79 281 N.D. 3) N-nitrosodimethylamine 0.00 74 •0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 .—.0 N.D. 15) 2,21-oxybis(1-Chloropropan 12.76 45 955' N.D. 16) 3&4-Methylphenol 0.00 108 N.D.

(#) = qualifier out of range (m) = manual integration 27765.D NP112701.M Thu Dec 20 11:22:46 2001 Page 1

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