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GCMS analysis results for sample AD27764, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27764 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033285–000033310

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27764.D Vial: 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Trimethylamine Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

5.61 0.42 ng/uL 105312 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trimethylamine 59 C3H9N 000075-50-3 56 2 Oxirane,/2,3-diethyl- 100 C6H120 004468-66-0 38 3 Trimet ylamine 59 C3H9N 000075-50-3 9 4 Trimet ylamine 59 C3H9N 000075-50-3 9 Abundance Scan 84 (5.610 min): 27764.D (-) m/z .58.10 100.00% 58 41

5000

67 85 A 5.20 5.40 5.60 — 5.80 6.00 f

.............................. — 1——— i "2 41.10 66.06% miz-> 10 20 30 40 50 60 70 80 90 100 Abundance #108: Trimethylamine 58

5000 42 ■ । ' i ■ 1 ■ ■ । । ' 1 • । 1 5.20 5.40 5.60 5.80 6.00 30 15 m/z 57.10 48.88% AL T 1—— ' — m/z-> 10 20 30 40 50 60 70 80 90 100 Abundance #1559: Oxirane, 2.3-diethyl- 41 58 .... ........ . 5.20 5.40 5.60__ 5.80 6.00 5000 m/ z 42.10 36.52%

85 । ‘ i • * ■ 1 i 1 ■ ' * i 67 72 100 ■ ■ ■ i ■ ’ ' ■ i • ■ ' ' i ' m/z--> 10 20 30 40 50 60 70 80 90 100 Abundance #62343: Trimethylamine 58 5.20 5.40 5.60 5.80 6.00 m/z 59.10 36.48% 5000- 42

30

i ■ ■ ■ ■ i ............................... I ■ ■ ■ ■ i ■ ■ 1 ' i 1 1 1 ■ i ' ■ ■ ■ i ' ■ ------- m/z-> 10 20 30 40 50 60 70 80 90 100 5.20 5.40 5.60 5.80 6.00

27764.D NP112701.M Thu Dec 20 11:43:26 2001 Page 4

NYC-WTC_000033297

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NYC-WTC_000033297Source: NYC Law Department, mirrored locally

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