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GCMS analysis results, sample AD27626, Jan 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis report for sample AD27626 identifying unknown compounds and 2,4-DDD quality control surrogate.

NYC-WTC_000033128–000033142

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1901\27626.D Vial: 16 Acq On : 20 Dec 2001 11:34 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 21 8:57 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Compound R.T. Qlon Response Cone Unit Qvalue

61) Benzidine 0.00 184 0 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 31.64 149 2992/ N.D. 65) Benzo(a)anthracene 33.18 228 N.D. 66) Bis(2-ethylhexyl)phthalate 33.42 149 12010 N.D. 67) Chrysene 33.18 228 3233 / N.D. 69) Di-n-Octylphthalate 35.64 149 (280 N.D. 70) Benzo(b)fluoranthene 0.00 252 —0 N.D. 71) Benzo(k)fluoranthene 0.00 252 0 N.D. 72) Benzo(a)pyrene 37.26 252 2790 N.D. 73) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 74) Dibenz(a,h)anthracene 0.00 278 0 N.D. 75) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 27626.D NP112701.M Fri Dec 21 08:57:30 2001 Page 3

NYC-WTC_000033132

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NYC-WTC_000033132Source: NYC Law Department, mirrored locally

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