Laboratory report documenting GCMS analysis of sample AD27288 conducted on December 19, 2001.
NYC-WTC_000032889–000032899Folder label: “GCMS X 11/14/01 A 12/12/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC1201\27288.D Vial: 8 Acq On : 12 Dec 2001 9:40 pm Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.
7.79 2.89 ng/uL 707728 1,4-Dichlorobenzene-d4 11.84
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 59 4 Acetie acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 Abundance Scan 322 (7.794 mln): 27288.D (-) m/z 43.10 100.00% 413
5000 59 101 7.40 7.60 7.80 '"I i । * i । 1 1 8.00 8.20 ---------32+ +53+ —Tu—mg 83 — m/z 44.77% 110 59.10
L miz-? 10 20 30 40 50 60 70 80 90 100 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43 5000 TTIT 59 7.40 7.60 7.80 8.00 8.20 m/z 18.25% 27 101 _____________________ ■ i__________ * • i * ' * * i ♦ ♦ * • i ‘ 1 1 1 r1 10 20 30 40 +49 r 1 T TB1T n-j 60 70 80 83 . 11 90 ! 100 ' ‘ 110 miz-> 50 Abundance #3245: 2-Pentanone, 4-hydraxy-4-methyl- 43 ■ i • ‘ ■ i ‘ rrr l 1 ' 1 b i 1 1 ‘ 1 i ■ ■ 7.40 7.60 7.80 8.00 8.20 5000 m/z 101.05 15.11% 59 ! 31 101 | 73 83 i - — —1 ‘ ‘ T-1 1 ' TI—nngr miz->____ 10 20 Abundance . ...... , > । T [-n-r-rj-r-r --------- 30 40 50 60 70 80 #64275:2-Pentanone, 4-hydroxy-4-methyl- 43 90 100 110 _L 7.40 7.60 7.80 8.00 8.20 m/z 41.10 6.25% 5000 59 15. 31 101 ------ * ! i ■ ' ' ■ i ■ ■ ■ ■ i 83 | ■ ' • ■ i • 1 • 1 i ■ ■ 1 ' i 1 IImI miz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00 8.20
27288.D NP112701.M Fri Dec 14 10:08:54 2001 Page 1
NYC-WTC_000032896
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NYC-WTC_000032389
Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032773
Laboratory report documenting GCMS analysis of environmental sample AD27189 conducted on December 11, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032378
Laboratory report for GCMS analysis of sample AD26984 completed on December 11, 2001, listing unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032847
Laboratory report documenting GCMS analysis of sample AD27232 conducted on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032492
Laboratory report for GCMS analysis of sample AD26993 completed on December 11, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032752
Laboratory report documenting GCMS analysis of environmental sample AD27118 conducted on December 11, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032481
Laboratory report for GCMS analysis of sample AD26992 completed on December 11, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032795
Laboratory report documenting GCMS analysis of environmental sample AD27191 conducted on December 11, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032909
Laboratory report documenting GCMS analysis of environmental sample AD27290 conducted on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032332
Laboratory report for GCMS analysis of sample AD26847 completed on December 11, 2001, documenting surrogate data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032321
Laboratory report for GCMS analysis of sample AD26346 completed on December 11, 2001, with surrogate recovery results.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032859
Laboratory report documenting GCMS analysis of sample AD27233 conducted on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000032814
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000032815
Header page from a GCMS data file listing method parameters and sample identifiers for December 2001 testing.
Filed in the same folder
NYC-WTC_000032818
Calibration data sheet for GCMS analysis using TCLP method, listing standards and response factors from December 2001.
Filed in the same folder
NYC-WTC_000032826
Log of GCMS analysis for sample AD27193 conducted on December 19, 2001, detecting other unknown compounds.
Filed in the same folder
NYC-WTC_000032837
Laboratory report documenting GCMS analysis of sample AD27194 performed on December 19, 2001, including detection of unknown compounds.
Filed in the same folder