GCMS calibration table for TCLP analysis, Dec 2001

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Data File : C:\HPCHEM\l\DATA\DEC1201\LB.D Vial: 2 Acq On : 12 Dec 2001 4:13 pm Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.79 2.30 ng/uL 948542 1,4-Dichlorobenzene-d4 11.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 74 2 2-Pentanone, 4 -hydroxy - 4 - me t hyl - 116 C6H1202 000123-42-2 59 3 2-Pentanone, 4-- hydroxy - 4 - methyl- 116 C6H1202 000123-42-2 43 4 Acetic acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 25 Abundance ( Scan 322 (7.792 min): LB.D (-) m/ z 43.05 100.00% I 43

5000 59

101 ITIIITT I 7.40 7.60 7.80 8.00 8.20 I 38,4 53 . 83 — । ■ • ■ > । ■ ■ • ■ । 1IH 50 60 i ' 1 70 ■ ■ i ' ‘ 80 ' i 90 m/z 59.10 48.24% m/z--> 10 20 30 40 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 1 i ' ' ' ■ i ■ ' ■ ‘ i

59 7.40 7.60 7.80 8.00 8.20 m/z 58.10 19.34% 15 31 101 I । 83 | Ui i ■ ■ ■ ■ i ' i ■ 1 ■ • i miz-s 10 20 30 40 50 60 70 80 90 100 110 'Abundance #64274; 2-Pentanone, 4-hydroxy-4-methyl- 43

7.40 7.60 7.80 8.00 8.20 5000 m/z 101.05 17.24% 59

27 . 83 101 । i 49 i ■ ■ • • i ■ ■ ' ■ i ' ■ ■ ■ i ■ i ■ ■ ■ ■ i miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- ■ i ' ■ • ■ i ■ 1 1 ’ i 1 43 7.40 7.60 7.80 8.00 8.20 m/ z 41.10 7.23% 5000 - 59

31 101 i ! — 73 83 - i ■ ' ' ' i ' ' ' ' i ' -I m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00 8.20

LB.D NP112701.M Fri Dec 14 10:09:39 2001 Page 1

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