GCMS analysis results for sample AD27188, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\27188.D Vial: 23 Acq On 8 Dec 2001 2:10 pm Operator: GALOS Sample gc/ms unknown 11/13 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.85 3.77 ng/uL •1107150 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4 -hydroxy-4-methyl - 116 C6H1202 000123-42-2 83 2 2-Pentanone, 4-hydroxy- 4-methyl- 116 C6H1202 000123-42-2 64 3 2 -Pentanone,/1-hydroxy-4 -methyl- 116 C6H1202 000123-42-2 59 4 Acetic acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 28 Abundance 7 Scan 328 (7.848 min): 27188.D (-) m/z 43.00 100 . 00% / 43

5000- 59

101 i ' ■ ■ ■ i

........................ 38, 1 53 , 83 — 7.40 7.60 7.80 8.00 8.20 ' ' I ' ■ ' ■ I ' ' ' •++ ' I ' ' ■ ' I 1 i ■ ■ ■ ■ i ' i m/z 59.10 44.57% m/z-> 10 20 30 40 50 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4R

5000 59 7.40 7.60 7.80 8.00 8.20 m/z 58.10 18.03% • ■ । ■ ■ ■ ■ । ■ • 27 : i ■ • .......... .. 49 TI L , 83 , .T — m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hycroxy-4-methyl- i 43

7.40 7.60 7.80 8.00 8.20 5000 - 59 m/z 101.0,5 14.85%

31 73 83 101 | TTL" I I i 1 1 ■ ' i ■ ' ■ ' i ' ' • ■ i ■ ' ■ ■ i ■ 1 ■ ■ i ' 1 1 1 I ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43 7.40 7.60 7.80 8.00 8.20 m/z 41.10 6.72% 5000 59

15 31 101 ____! । i 83 i ■ • ■ ■ I 1 1 1 1 I1 | 1 1 • • । ■ i ■ ‘ ' i ' ' ' ' i ' ■ ' ■ i - —IT*.PP11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00 8.20

27188.D NP112701.M Tue Dec 11 15:13:04 2001 Page 1

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