GCMS results log, sample AD27056, Dec 10 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\DEC0501\27055.D Vial: 10 Acq On 5 Dec 2001 5:11 pm Operator: GALOS Sample gc/ms unknown 11/13 1 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 10:31 2001 Quant Results File: NP112701.RES Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.87 152 1098487 20.00 ng/uL -0.07 19) Naphthalene-d8 15.48 136 4154790 20.00 ng/uL -0.07 31) Acenaphthene-diO 20.75 164 1860510 20.00 ng/uL -0.07 49) Phenanthrene-diO 25.31 188 50902 20.00 ng/uL 0.07 59) Chrysene-dl2 33.17 240 1606018 20.00 ng/uL -0.08 68) Perylene-dl2 37.26 264 1096339 20.00 ng/uL -0.08 System Monitoring Compounds 4) 2 - Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75 - 000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.87 132 1007 0.01 ng/uL 0.44 Soiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2 -Dichlorobenzene-d4 12.21 152 2 97 0.01 ng/uL -0.24 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Soiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2 - Fluorobiphenyl 18.91 172 1924 0.02 ng/uL 0.08 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked .Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Soiked .Amount 50.000 Range 58 98 Recovery = 0.00%# Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis ( 2-Chloroethyl) ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1, 3 - Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2 , 2 1 -oxybis ( 1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nicrosodi-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 22) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#' = qualifier out of range (m) = manual integration 27055.D NP112701M Fri Dec 07 10:35:19 2001 Page 1

NYC-WTC_000032629