GCMS results log, sample AD27055, Dec 10 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\1\DATA\DEC0501\27015 .D Vial: 9 Acq On 5 Dec 2001 4:17 pm Operator: GALOS Sample gc/ms unknown 11/13 4 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 10:31 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.87 152 1161836 20.00 ng/uL -0.06 19) Naphthalen:-d8 15.48 136 4405206 20.00 ng/uL -0.06 31) Acenaphthene-diO 20.76 164 1993775 20.00 ng/uL -0.06 49) Phenanthrene-diO 25.17 188 2788301 2 0.00 ng/uL -0.07 59) Chrysene-d12 33.17 240 1642818 20.00 ng/uL -0.07 68) Perylene-dl2 37.25 264 1107550 20.00 ng/uL -0.08

System Monitoring Compounds 4) 2 - Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.87 132 939 0.01 ng/uL 0.45 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1, 2 -Dichlorobenzene-d4 12.18 152 608 0.01 ng/uL -0.28 Spiked .Amount 50.000 Range 26 73 Recovery = 0.02%# 2 0) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked .Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2 - Fluorobiphenyl 18.91 172 1933 0.02 ng/uL 0.07 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33 ) 2,4, 6 - Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1, 2-Dichlcrobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitrosodi-n - propylamine 0.00 70 0 N.D. 18) Hexachlorcethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 ' 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 27015. D 1P112701.M Fri Dec 07 10:35:04 2001 Page 1

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