GCMS method parameters and calibration data, Nov-Dec 2001

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\l\DATA\DEC0501\DFTPP. D Vial: 1 Acq On 5 Dec 2001 8:46 am Operator: GALOS Sample Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table

Abundance TIC: DFTPP.D 1e+07-

: 8000000

6000000 1 ' 4000000

| 2000000

s' , 4 I ......... 1 ....... .T l .. 1 1 i IO J , Time-> 24.40 24.60 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 Abundance Average of 26.370 to 26.416 min.: DFTPP.D 198 442 • 600000

I 400000 69 127 51 255 110 200000 275 224 93

miz-> 0—38+4+ 40 J । 148 1671 r"h +4 -*—* —4 * 1 r +4 60 80 — 1 4422 — 4— — n । 11 28310323336,352305 n mPPPP 383,403 ■ -----42. ITr 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.370 to 26.416 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 45.4 305979 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 60.7 408881 PASS 70 69 0.00 2 0.4 1589 PASS 127 198 40 60 50.1 337435 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 673916 PASS 199 198 5 9 6.5 43946 PASS 275 198 10 30 20.4 137168 PASS 365 198 1 99 2.9 19581 PASS 441 443 1 99 81.2 106161 PASS 442 198 40 110 99.8 672341 PASS 443 442 17 23 -19.4 130693 PASS

DFTPP.D NP112701.M Tue Dec 11 08:08:25 2001

NYC-WTC_000032590