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GCMS results log, sample AD26346, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26346 completed on December 11, 2001, with surrogate recovery results.

NYC-WTC_000032321–000032331

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\26846.D Vial: 30 Acq On 7 Dec 2001 1:30 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.050 16 23 32 rVB 106582 212695 1.94% 0.374% 2 7.856 325 329 347 rBV 600469 1248218 11.41% 2.192% 3 11.891 763 769 788 rBV 4232178 8630922 78.89% 15.159% 4 15.504 1156 1163 1180 rBV 4947012 10940593 100.00% 19.215% 5 20.777 1731 1738 1772 rBV 5179583 10841753 99.10% 19.042%

6 25.187 2212 2219 2230 rBV2 4781324 10166688 92.93% 17.856% 7 33.193 3085 3092 3109 rBV2 3575372 8053003. 73.61% 14.144% 8 37.283 3529 3538 3562 rBV2 2470631 6843265 62.55% 12.019%

Sum of corrected areas: 56937137

26846.D NP112701.M Tue Dec 11 14:47:41 2001

NYC-WTC_000032327

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NYC-WTC_000032327Source: NYC Law Department, mirrored locally

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