Analysis report dated December 31, 2001, identifying bis(2-Ethylhexyl)phthalate and 1,1,2,2-Tetrachloroethane in sample AD26710.
NYC-WTC_000032114–000032127Folder label: “GCMS X 11/7/01 A 12/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\DEC0501\26710.D Vial: 4 Acq On 5 Dec 2001 11:29 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 9:59 2001 Quant Results File: NP112701.RES Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.87 152 1102708 20.00 ng/uL -0.06 19) Naphthalene-d8 15.48 136 4173227 20.00 ng/uL -0.07 31) Acenaphthene-diO 20.75 164 1881191 20.00 ng/uL -0.07 49) Phenanthrene-diO 25.16 188 2684704m 20.00 ng/uL -0.08 59) Chrysene-dl2 33.17 240 1711905 20.00 ng/uL -0.08 68) Perylene-dl2 37.25 264 1076556 20.00 ng/uL -0.09
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.87 132 616 0.01 ng/uL 0.44 Spiked Amount 75,000 Range 3 4 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 12.20 152 583 0.01 ng/uL -0.26 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.91 172 2034 0.02 ng/uL 0.08 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%# Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.0 0 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 12.87 45 2424 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 26710.D NP112701.M Fri Dec 07 10: 0:07 2001 Page 1
NYC-WTC_000032116
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NYC-WTC_000031905
Laboratory report documenting GCMS analysis of sample AD26624 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032128
Laboratory report documenting GCMS analysis of sample AD26711 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031889
GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031788
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 0.72 ug/L in sample AD26533.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031762
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 0.80 ug/L in sample AD26532.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031775
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 0.72 ug/L in sample AD26533.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031801
Mass spectrometry analysis of sample AD26534 detected 1,1,2,2-Tetrachloroethane at 2.9 ug/L with 93% fit confidence, Dec 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032142
Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031814
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 3.4 ug/L in sample AD2653S.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032079
Laboratory report documenting GCMS analysis of sample AD26681 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031831
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 3.2 ug/L in sample AD26536.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031372
Analysis report for sample AD26335 indicating the presence of other unknown compounds on December 4, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000031869
Illegible text on a single page from the GCMS folder covering November to December 2001.
Filed in the same folder
NYC-WTC_000031870
Index or cover sheet page for the GCMS folder covering the period from November 7 to December 6, 2001.
Filed in the same folder
NYC-WTC_000031876
Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.
Filed in the same folder
NYC-WTC_000031889
GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.
Filed in the same folder
NYC-WTC_000031905
Laboratory report documenting GCMS analysis of sample AD26624 identifying unknown compounds on December 10, 2001.
Filed in the same folder