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GCMS analysis results for sample AD26679, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26679 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032028–000032057

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: GALOS Date Acquired: 4 Dec 2001 2:27 pm Data File: C:\HPCHEM\l\DATA\DEC0401\26679.D Name: gc/ms unknown Mise: Method: C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title: 208 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Hydrogen azide 4.98 0.7 ng/uL 223997 ISTD01 11.86 6833660 20.0 Cyelohexane , me t hyl - 5.03 0.9 ng/uL 316118 ISTD01 11.86 6833660 20.0 Oxepane , 2,2,4-trime 5.13 1.2 ng/uL 394038 ISTD01 11.86 6833660 20.0 Oxirane, ■ 3 - ethyl -2,2 5.20 1.9 ng/uL 656818 ISTD01 11.86 6833660 20.0 Propanoic’ acid, 2-me 6.12 1.2 ng/uL 427042 ISTD01 11.86 6833660 20.0 3-=Hexanone 6.47 0.5 ng/uL 159595 ISTDOl 11.86 6833660 20.0 2-Hexanone 6.57 0.5 ng/uL 171766 ISTDOl 11.86 6833660 20.0 3-Hexanol 6.70 0.4 ng/uL 149870 ISTDOl 11.86 6833660 20.0 2 -Butanol , 3 -methyl - 7.17 5.4 ng/uL 1829250 ISTDOl 11.86 6833660 2 0.0 2 -Pentanone , 4 - hydro 7.83 7.7 ng/uL 2623390 ISTDOl 11.86 6833660 20.0 Hexane, 2 -me thyl- 10.30 1.5 ng/uL 523896 ISTDOl 11.86 68.33660 20.0 Oxirane, 2-methyl-3- 10.51 0.7 ng/uL 247655 ISTDOl 11.86 6833660 20.0 1 Hexene, 2 -methyl- 29.57 1.3 ng/uL 275824 ISTD05 33.17 4253720 20.0 Eicosane 30.75 0.5 ng/uL 109062 ISTD05 33.17 4253720 20.0 Pent adecane, 8 - me t hy 31.70 0.7 ng/uL 159172 ISTD05 33.17 4253720 20.0 Nonadecane 31.79 1.3 ng/uL 269486 ISTD05 33.17 4253720 20.0 Eicosane 32.78 1.0 ng/uL 206979 ISTD05 33.17 4253720 20.0 10-Methylnonadecane 33.73 1.1 ng/uL 233623 ISTD05 33.17 4253720 20.0 Dotriacontane 34.64 0.6 ng/uL 132056 ISTD05 33.17 4253720 20.0 Dotri acontane__ 35.53 0.6 ng/uL 92458 ISTD06 37.25 2845820 20.0

26679.D NP112701.M Fri Dec 07 13:10:39-2001

NYC-WTC_000032056

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NYC-WTC_000032056Source: NYC Law Department, mirrored locally

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