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GCMS analysis results for sample AD26626, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26626 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031940–000031967

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.013 14 19 26 rBV 149751 460587 6.12% 1.003% 2 5.105 26 29 33 rW 176874 344175 4.57% 0.750% 3 5.169 33 36 57 rVB 273031 821996 10.91% 1.790% 4 5.655 86 89 106 rVB2 97930 168860 2.24% 0.368% 5 6.113 135 139 154 rBV 164993 449470 5.97% 0.979%

6 6.462 172 177 184 rBV 67280 155276 2.06% 0.338% 7 6.572 185 189 199 rVB 69763 157980 2.10% 0.344% 8 6.700 199 203 205 rBV 64453 119802 1.59% 0.261% 9 6.819 212 216 22 0 rW 41816 83134 1.10% 0.181% 10 7.168 249 254 267 rBV 924193 1813581 24.08% 3.950%

11 7.837 323 327 346 rBV 1169606 2483034 32.97% 5.408% 12 10.313 593 597 607 rBV 241129 530242 7.04% 1.155% 13 10.524 615 620 630 rBV 125995 264787 3.52% 0.577% 14 11.891 763 769 782 rBV 2830089 6159217 81.78% 13.415% 15 15.504 1157 1163 1180 rBV 3471824 7531301 100.00% 16.404%

16 20.776 1731 1738 1754 rBV 3578973 7448097 98.90% 16.223% 17 25.187 2212 2219 2230 rBV2 2954995 6554402 87.03% 14.276% 18 2 9.58 9' 2694 2699 2707 rBV 363283 711019 9.44% 1.549% 19 29.699 2707 2711 2718 rVB2 43513 93226 1.24% 0.203% 20 30.772’ 2823 2828 2836 rVB 45125 94535 1.26% 0.206%

21 31.716 2925 2931 2936 rBV 192553 428441 5.69% 0.933% 22 31.808 2936 2941 2951 rVB 117251 281263 3.73% 0.613% 23 32.798 3044 3049 3057 rBV 78958 196701 2.61% 0.428% 24 33.183 3085 3091 3103 rBV2 2019825 4500054 59.75% 9.802% 25 33.449 3116 3120 3131 rVB 38408 94033 1.25% 0.205%

26 33.752 3147 3153 3164 rBV 83292 232841 3.09% 0.507% 27 34.669 3247 3253 3266 rBV 39606 125742 1.67% 0.274% 28 35.549 3344 3349 3361 rBV 28629 108155 1.44% 0.236%

NYC-WTC_000031943

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NYC-WTC_000031943Source: NYC Law Department, mirrored locally

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