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GCMS analysis report for sample AD26474, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26474 noting other unknown compounds.

NYC-WTC_000031650–000031660

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document ' Am Detri ewed)

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3001\26474.D Acq On : 30 NOV 2001 6:35 pm Vial: 8 Sample : gc/ms unknown 11/3 Operator: GALOS Mise Inst : GC/MS Ins MS Integration Params: RTEINT.P Multiplr: 1.00 Quant Time: Dec 3 14:54 2001 Quant Results File: NP112701.RES Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Last Update Wed Nov 28 15:33:44 2001 Response via Initial Calibration DataAcq Meth NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.89 152 1602448 20.00 ng/uL 19) Naphthalene-d8 -0.05 15.50 136 6302486 20.00 ng/uL -0.05 31) Acenaphthene-diO 20.78 164 2840919 20.00 ng/uL 49) Phenanthrene-diO -0.05 25.19 188 4068080 20.00 ng/uL -0.05 59) Chrysene-dl2 33.19 240 2553033 68) Perylene-dl2 20.00 ng/uL -0.05 37.28 264 1861467 20.00 ng/uL -0.05 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 Spiked Amount 0.00 ng/uL 75.000 Range 18 - 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 Spiked Amount 0 0.00 ng/uL 75.000 Range 19 - 32 Recovery 6) 2-Chlorophenol-d4 = 0.00%# 11.89 132 1408 0.01 ng/uL 0.47 Spiked Amount 75.000 Range 34 - 84 7) 1,2-ichlorobenzene-d4 Recovery = 0.01%# Spiked Amount 12.40 152 16545 0.24 ng/uL -0.05 50.000 Range 26 - 73 Recovery 20) Nitrobenzene-d5 = 0.48%# 0.00 82 0 0.00 ng/uL Spiked mmount 50.000 Range 55 98 32) 2-Fliorobiphenyl Recovery = 0.00%# 18.92 172 5572 0.03 ng/uL 0.09 Spiked mount 50.000 Range: 42 78 33) 2,4, Tribromophenol Recovery = 0.06%# 0.00 330 0 0.00 ng/uL Spiked mount 75.000 Range 45 96 62) Terpenyl-d14 Recovery = 0.00%# 0.00 244 0 0.00 ng/uL Spiked mount 50.000 Range 58 98 Recovery = 0.00%# Target Copounds 2) Pyriine 0.00 Qvalue 79 0 N.D. 3) N-nirosodimethylamine 0.00 74 0 N.D. 8) Phen- 0.00 94 9) bis (-Chloroethyl) ether 0 N.D. 0.00 93 0 N.D. 10) 2-Chrophenol 0.00 128 0 N.D. 11) 1, 3--chlorobenzene 0.00 146 0 12) 1,4 -chlorobenzene N.D. 0.00 146 0 N.D. 13) 1,2-chlorobenzene 0.00 146 0 14) 2-Meylphenol N.D. 0.00 108 0 N.D. 15) 2,2’«ybis(l-chloropropan 0.00 45 0 16) 3 &4 -thylphenol N.D. 0.00 108 0 N.D. 17) N-Niosodi-n-propylamine 0.00 70 18) Hexaloroethane 0 N.D. 0.00 117 0 21) Nitrenzene 0.00 77 0 N.D. N.D. 22) Isotone 0.00 82 0 N.D. 2 (#) = quaier out of range (m) = manual integration 26474.D 112701.M Tue Dec 04 08:23:29 2001 Page 1

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NYC-WTC_000031652Source: NYC Law Department, mirrored locally

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